Sb@Ni-12@Sb-20(-/+) and Sb@Pd-12@Sb-20(n) Cluster Anions, Where n =+1,-1,-3,-4: Multi-Oxidation-State Clusters of Interpenetrating Platonic Solids

Wang, Y; Moses-DeBusk, M; Stevens, L; Hu, JK; Zavalij, P; Bowen, K; Dunlap, BI; Glaser, ER; Eichhorn, B

Eichhorn, B (reprint author), Univ Maryland, Dept Chem & Biochem, College Pk, MD 20742 USA.

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2017; 139 (2): 619

Abstract

K5Sb4 and K3Sb7 Zintl ion precursors react with Pd(PPh3)(4) in ethylenediamine/toluene/PBu4+ solutions to give crystals of Sb@Pd-12@Sb-20(n-)/PBu4+ sa......

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