One-Step, Gram-Scale Synthesis of Caffeine-d9 from Xanthine and CD3I

Tarasca, MV; Tomlinson, CJ; Gris, P; Murphy, GK

Murphy, GK (通讯作者)，Dept Chem, 200 Univ Ave W, Waterloo, ON N2L3G1, Canada.;Murphy, GK (通讯作者)，Waterloo Inst Nanotechnol, 200 Univ Ave W, Waterloo, ON N2L3G1, Canada.;Gris, P (通讯作者)，deutraMed, 40 Sanford Fleming Dr, Collingwood, ON L9Y4V7, Canada.

SYNTHESIS-STUTTGART, 2023; 55 (5): 821

Abstract

A one-step, gram-scale synthesis of caffeine-d9 was achieved using xanthine and CD3I. The reaction proceeds at room temperature using dimsyl sodium as......

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