Safe Scale-Up of an N-Bromosuccinimide Involved Bromination Reaction

Guan, MX; Tian, YT; Zhao, JB; Gu, XX; Jiang, XG; Wang, XF; Zhang, YB; Zhang, XM

Zhang, XM (corresponding author), Suzhou Novartis Tech Dev Co Ltd, Chem & Analyt Dev, Changshu 215537, Jiangsu, Peoples R China.

ORGANIC PROCESS RESEARCH & DEVELOPMENT, 2021; 25 (6): 1375

Abstract

Y A hazardous side reaction between N-bromosuccinimide (NBS) and 2-methyltetrahydrofuran (2-MeTHF) was identified during the thermal safety analysis t......

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