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J Endod：加热时间和温度对环氧树脂以及硅酸钙类封闭剂的影响

2017-10-19 lishiting MedSci原创

热熔充填根管封闭剂适应性
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随着牙髓治疗中热熔充填技术的不断应用，学者们更多的兴趣集中到热熔时封闭剂适应性的变化上。这篇研究是通过化学和热重分析法评估热应用持续时间及温度对环氧树脂和硅酸钙类封闭剂的影响。

随着牙髓治疗中热熔充填技术的不断应用，学者们更多的兴趣集中到热熔时封闭剂适应性的变化上。这篇研究是通过化学和热重分析法评估热应用持续时间及温度对环氧树脂和硅酸钙类封闭剂的影响。研究将每种新混合的封闭剂样本(n = 5/组)加热至200°C或250°C 30或60秒。另准备2份样本在混合或充填后不施加热暴露的情况下直接接受检测。使用拉曼光谱鉴定材料的化学结构改变，并通过2-way方差分析比较发生变化的可测定峰值。除此之外，当温度以20°C/min的速率加热至250°C时(持续11分钟)或维持在37°C 8小时的时候，通过热重分析法(TGA)评估加热对质量变化的影响。结果显示，在不同组硅酸钙样本的所有光谱中未发现明显差异，而TGA在250°C和37°C时分别表现出15%和18%的失重。当加热60秒时，树脂类封闭剂样本展现出明显的差异，包括未固化树脂内的苯环键和芳香胺。TGA结果显示，温度加热至250°C和37°C时，封闭剂质量仅有轻度改变，分别为1.2%和1.8%。结论：热应用持续时间和温度会影响环氧树脂封闭剂的化学结构。为此，当使用热熔垂直加压充填时，需要考虑到根管封闭适应性以及热应用持

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    2018-08-06 ms1948154235210413

    #环氧树脂#

    0

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    2018-05-13 szhvet

    #硅酸钙#

    0

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    2017-10-21 12498dd9m12暂无昵称

    #封闭剂#

    0

  4. [GetPortalCommentsPageByObjectIdResponse(id=1798177, encodeId=c2811e98177f0, content=<a href='/topic/show?id=02e068505b7' target=_blank style='color:#2F92EE;'>#环氧树脂#</a>, beContent=null, objectType=article, channel=null, level=null, likeNumber=33, replyNumber=0, topicName=null, topicId=null, topicList=[TopicDto(id=68505, encryptionId=02e068505b7, topicName=环氧树脂)], attachment=null, authenticateStatus=null, createdAvatar=https://thirdwx.qlogo.cn/mmopen/vi_32/Bnia2EtH2IvyBtniaWHPQOYAicsN3IAL1ZuPV7qyALcdCiawRJdEiafMxWTxzERQW7eeKg8HfCKCRK2CJicy073C4RJg/132, createdBy=464b2500186, createdName=ms1948154235210413, createdTime=Mon Aug 06 14:56:00 CST 2018, time=2018-08-06, status=1, ipAttribution=), GetPortalCommentsPageByObjectIdResponse(id=1705285, encodeId=28761e05285d6, content=<a href='/topic/show?id=4394e351421' target=_blank style='color:#2F92EE;'>#硅酸钙#</a>, beContent=null, objectType=article, channel=null, level=null, likeNumber=27, replyNumber=0, topicName=null, topicId=null, topicList=[TopicDto(id=73514, encryptionId=4394e351421, topicName=硅酸钙)], attachment=null, authenticateStatus=null, createdAvatar=null, createdBy=933b30968945, createdName=szhvet, createdTime=Sun May 13 17:56:00 CST 2018, time=2018-05-13, status=1, ipAttribution=), GetPortalCommentsPageByObjectIdResponse(id=1443035, encodeId=8608144303551, content=<a href='/topic/show?id=674546e8323' target=_blank style='color:#2F92EE;'>#封闭剂#</a>, beContent=null, objectType=article, channel=null, level=null, likeNumber=0, replyNumber=0, topicName=null, topicId=null, topicList=[TopicDto(id=46783, encryptionId=674546e8323, topicName=封闭剂)], attachment=null, authenticateStatus=null, createdAvatar=null, createdBy=b88a5021004, createdName=12498dd9m12暂无昵称, createdTime=Sat Oct 21 13:56:00 CST 2017, time=2017-10-21, status=1, ipAttribution=), GetPortalCommentsPageByObjectIdResponse(id=1627560, encodeId=8b4a162e56068, content=<a href='/topic/show?id=cea46199eba' target=_blank style='color:#2F92EE;'>#树脂#</a>, beContent=null, objectType=article, channel=null, level=null, likeNumber=31, replyNumber=0, topicName=null, topicId=null, topicList=[TopicDto(id=61997, encryptionId=cea46199eba, topicName=树脂)], attachment=null, authenticateStatus=null, createdAvatar=null, createdBy=378b21121654, createdName=chenshujs, createdTime=Sat Oct 21 13:56:00 CST 2017, time=2017-10-21, status=1, ipAttribution=), GetPortalCommentsPageByObjectIdResponse(id=254875, encodeId=11a32548e5fa, content=学习一下谢谢分享, beContent=null, objectType=article, channel=null, level=null, likeNumber=45, replyNumber=0, topicName=null, topicId=null, topicList=[], attachment=null, authenticateStatus=null, createdAvatar=https://wx.qlogo.cn/mmopen/jW482SpianMayicTRbRZ5RzaiabIFicf63hKvVMjL6aJlx4yX4UcXmzX9DyibCRcicq0QtCRWMaQKh8MYjE1D3EKUBopgiaGWYuqbeR/0, createdBy=0c2b1999806, createdName=三生有幸9135, createdTime=Sat Oct 21 12:50:44 CST 2017, time=2017-10-21, status=1, ipAttribution=), GetPortalCommentsPageByObjectIdResponse(id=254465, encodeId=9e00254465cb, content=谢谢分享, beContent=null, objectType=article, channel=null, level=null, likeNumber=57, replyNumber=0, topicName=null, topicId=null, topicList=[], attachment=null, authenticateStatus=null, createdAvatar=https://wx.qlogo.cn/mmopen/Pw2csslt7CukWiabqiblnQAXaDEiaxhu025c3P0XshccTrbvGWBjKvnHIxbK3vqa80P7WGIFuicCFet97TicrNKpgB3TdabxP1vMh/0, createdBy=28851960965, createdName=榄枷檬, createdTime=Fri Oct 20 07:01:49 CST 2017, time=2017-10-20, status=1, ipAttribution=), GetPortalCommentsPageByObjectIdResponse(id=254438, encodeId=c38d254438a2, content=学习了新知识.受益, beContent=null, objectType=article, channel=null, level=null, likeNumber=51, replyNumber=0, topicName=null, topicId=null, topicList=[], attachment=null, authenticateStatus=null, createdAvatar=https://cdnapi.center.medsci.cn/medsci/head/2017/08/29/bbc5cc0eed9b8d17623d2fd49dbdf19a.jpg, createdBy=79522135794, createdName=yjs木玉, createdTime=Fri Oct 20 05:46:28 CST 2017, time=2017-10-20, status=1, ipAttribution=), GetPortalCommentsPageByObjectIdResponse(id=254433, encodeId=d3b3254433d4, content=使用热熔垂直加压充填时.需要考虑到根管封闭适应性以及热应用持续时间., beContent=null, objectType=article, channel=null, level=null, likeNumber=59, replyNumber=0, topicName=null, topicId=null, topicList=[], attachment=null, authenticateStatus=null, createdAvatar=https://cdnapi.center.medsci.cn/medsci/head/2017/04/24/1c2dbd6706e64df33befd6663f1d6b37.jpg, createdBy=94f61661779, createdName=lyh994, createdTime=Fri Oct 20 02:23:38 CST 2017, time=2017-10-20, status=1, ipAttribution=), GetPortalCommentsPageByObjectIdResponse(id=254411, encodeId=e654254411b7, content=不错的视频值得推荐一下, beContent=null, objectType=article, channel=null, level=null, likeNumber=51, replyNumber=0, topicName=null, topicId=null, topicList=[], attachment=null, authenticateStatus=null, createdAvatar=, createdBy=04f22055142, createdName=131****2916, createdTime=Thu Oct 19 23:03:06 CST 2017, time=2017-10-19, status=1, ipAttribution=)]
    2017-10-21 chenshujs

    #树脂#

    0

  5. [GetPortalCommentsPageByObjectIdResponse(id=1798177, encodeId=c2811e98177f0, content=<a href='/topic/show?id=02e068505b7' target=_blank style='color:#2F92EE;'>#环氧树脂#</a>, beContent=null, objectType=article, channel=null, level=null, likeNumber=33, replyNumber=0, topicName=null, topicId=null, topicList=[TopicDto(id=68505, encryptionId=02e068505b7, topicName=环氧树脂)], attachment=null, authenticateStatus=null, createdAvatar=https://thirdwx.qlogo.cn/mmopen/vi_32/Bnia2EtH2IvyBtniaWHPQOYAicsN3IAL1ZuPV7qyALcdCiawRJdEiafMxWTxzERQW7eeKg8HfCKCRK2CJicy073C4RJg/132, createdBy=464b2500186, createdName=ms1948154235210413, createdTime=Mon Aug 06 14:56:00 CST 2018, time=2018-08-06, status=1, ipAttribution=), GetPortalCommentsPageByObjectIdResponse(id=1705285, encodeId=28761e05285d6, content=<a href='/topic/show?id=4394e351421' target=_blank style='color:#2F92EE;'>#硅酸钙#</a>, beContent=null, objectType=article, channel=null, level=null, likeNumber=27, replyNumber=0, topicName=null, topicId=null, topicList=[TopicDto(id=73514, encryptionId=4394e351421, topicName=硅酸钙)], attachment=null, authenticateStatus=null, createdAvatar=null, createdBy=933b30968945, createdName=szhvet, createdTime=Sun May 13 17:56:00 CST 2018, time=2018-05-13, status=1, ipAttribution=), GetPortalCommentsPageByObjectIdResponse(id=1443035, encodeId=8608144303551, content=<a href='/topic/show?id=674546e8323' target=_blank style='color:#2F92EE;'>#封闭剂#</a>, beContent=null, objectType=article, channel=null, level=null, likeNumber=0, replyNumber=0, topicName=null, topicId=null, topicList=[TopicDto(id=46783, encryptionId=674546e8323, topicName=封闭剂)], attachment=null, authenticateStatus=null, createdAvatar=null, createdBy=b88a5021004, createdName=12498dd9m12暂无昵称, createdTime=Sat Oct 21 13:56:00 CST 2017, time=2017-10-21, status=1, ipAttribution=), GetPortalCommentsPageByObjectIdResponse(id=1627560, encodeId=8b4a162e56068, content=<a href='/topic/show?id=cea46199eba' target=_blank style='color:#2F92EE;'>#树脂#</a>, beContent=null, objectType=article, channel=null, level=null, likeNumber=31, replyNumber=0, topicName=null, topicId=null, topicList=[TopicDto(id=61997, encryptionId=cea46199eba, topicName=树脂)], attachment=null, authenticateStatus=null, createdAvatar=null, createdBy=378b21121654, createdName=chenshujs, createdTime=Sat Oct 21 13:56:00 CST 2017, time=2017-10-21, status=1, ipAttribution=), GetPortalCommentsPageByObjectIdResponse(id=254875, encodeId=11a32548e5fa, content=学习一下谢谢分享, beContent=null, objectType=article, channel=null, level=null, likeNumber=45, replyNumber=0, topicName=null, topicId=null, topicList=[], attachment=null, authenticateStatus=null, createdAvatar=https://wx.qlogo.cn/mmopen/jW482SpianMayicTRbRZ5RzaiabIFicf63hKvVMjL6aJlx4yX4UcXmzX9DyibCRcicq0QtCRWMaQKh8MYjE1D3EKUBopgiaGWYuqbeR/0, createdBy=0c2b1999806, createdName=三生有幸9135, createdTime=Sat Oct 21 12:50:44 CST 2017, time=2017-10-21, status=1, ipAttribution=), GetPortalCommentsPageByObjectIdResponse(id=254465, encodeId=9e00254465cb, content=谢谢分享, beContent=null, objectType=article, channel=null, level=null, likeNumber=57, replyNumber=0, topicName=null, topicId=null, topicList=[], attachment=null, authenticateStatus=null, createdAvatar=https://wx.qlogo.cn/mmopen/Pw2csslt7CukWiabqiblnQAXaDEiaxhu025c3P0XshccTrbvGWBjKvnHIxbK3vqa80P7WGIFuicCFet97TicrNKpgB3TdabxP1vMh/0, createdBy=28851960965, createdName=榄枷檬, createdTime=Fri Oct 20 07:01:49 CST 2017, time=2017-10-20, status=1, ipAttribution=), GetPortalCommentsPageByObjectIdResponse(id=254438, encodeId=c38d254438a2, content=学习了新知识.受益, beContent=null, objectType=article, channel=null, level=null, likeNumber=51, replyNumber=0, topicName=null, topicId=null, topicList=[], attachment=null, authenticateStatus=null, createdAvatar=https://cdnapi.center.medsci.cn/medsci/head/2017/08/29/bbc5cc0eed9b8d17623d2fd49dbdf19a.jpg, createdBy=79522135794, createdName=yjs木玉, createdTime=Fri Oct 20 05:46:28 CST 2017, time=2017-10-20, status=1, ipAttribution=), GetPortalCommentsPageByObjectIdResponse(id=254433, encodeId=d3b3254433d4, content=使用热熔垂直加压充填时.需要考虑到根管封闭适应性以及热应用持续时间., beContent=null, objectType=article, channel=null, level=null, likeNumber=59, replyNumber=0, topicName=null, topicId=null, topicList=[], attachment=null, authenticateStatus=null, createdAvatar=https://cdnapi.center.medsci.cn/medsci/head/2017/04/24/1c2dbd6706e64df33befd6663f1d6b37.jpg, createdBy=94f61661779, createdName=lyh994, createdTime=Fri Oct 20 02:23:38 CST 2017, time=2017-10-20, status=1, ipAttribution=), GetPortalCommentsPageByObjectIdResponse(id=254411, encodeId=e654254411b7, content=不错的视频值得推荐一下, beContent=null, objectType=article, channel=null, level=null, likeNumber=51, replyNumber=0, topicName=null, topicId=null, topicList=[], attachment=null, authenticateStatus=null, createdAvatar=, createdBy=04f22055142, createdName=131****2916, createdTime=Thu Oct 19 23:03:06 CST 2017, time=2017-10-19, status=1, ipAttribution=)]
    2017-10-21 三生有幸9135

    学习一下谢谢分享

    0

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    2017-10-20 榄枷檬

    谢谢分享

    0

  7. [GetPortalCommentsPageByObjectIdResponse(id=1798177, encodeId=c2811e98177f0, content=<a href='/topic/show?id=02e068505b7' target=_blank style='color:#2F92EE;'>#环氧树脂#</a>, beContent=null, objectType=article, channel=null, level=null, likeNumber=33, replyNumber=0, topicName=null, topicId=null, topicList=[TopicDto(id=68505, encryptionId=02e068505b7, topicName=环氧树脂)], attachment=null, authenticateStatus=null, createdAvatar=https://thirdwx.qlogo.cn/mmopen/vi_32/Bnia2EtH2IvyBtniaWHPQOYAicsN3IAL1ZuPV7qyALcdCiawRJdEiafMxWTxzERQW7eeKg8HfCKCRK2CJicy073C4RJg/132, createdBy=464b2500186, createdName=ms1948154235210413, createdTime=Mon Aug 06 14:56:00 CST 2018, time=2018-08-06, status=1, ipAttribution=), GetPortalCommentsPageByObjectIdResponse(id=1705285, encodeId=28761e05285d6, content=<a href='/topic/show?id=4394e351421' target=_blank style='color:#2F92EE;'>#硅酸钙#</a>, beContent=null, objectType=article, channel=null, level=null, likeNumber=27, replyNumber=0, topicName=null, topicId=null, topicList=[TopicDto(id=73514, encryptionId=4394e351421, topicName=硅酸钙)], attachment=null, authenticateStatus=null, createdAvatar=null, createdBy=933b30968945, createdName=szhvet, createdTime=Sun May 13 17:56:00 CST 2018, time=2018-05-13, status=1, ipAttribution=), GetPortalCommentsPageByObjectIdResponse(id=1443035, encodeId=8608144303551, content=<a href='/topic/show?id=674546e8323' target=_blank style='color:#2F92EE;'>#封闭剂#</a>, beContent=null, objectType=article, channel=null, level=null, likeNumber=0, replyNumber=0, topicName=null, topicId=null, topicList=[TopicDto(id=46783, encryptionId=674546e8323, topicName=封闭剂)], attachment=null, authenticateStatus=null, createdAvatar=null, createdBy=b88a5021004, createdName=12498dd9m12暂无昵称, createdTime=Sat Oct 21 13:56:00 CST 2017, time=2017-10-21, status=1, ipAttribution=), GetPortalCommentsPageByObjectIdResponse(id=1627560, encodeId=8b4a162e56068, content=<a href='/topic/show?id=cea46199eba' target=_blank style='color:#2F92EE;'>#树脂#</a>, beContent=null, objectType=article, channel=null, level=null, likeNumber=31, replyNumber=0, topicName=null, topicId=null, topicList=[TopicDto(id=61997, encryptionId=cea46199eba, topicName=树脂)], attachment=null, authenticateStatus=null, createdAvatar=null, createdBy=378b21121654, createdName=chenshujs, createdTime=Sat Oct 21 13:56:00 CST 2017, time=2017-10-21, status=1, ipAttribution=), GetPortalCommentsPageByObjectIdResponse(id=254875, encodeId=11a32548e5fa, content=学习一下谢谢分享, beContent=null, objectType=article, channel=null, level=null, likeNumber=45, replyNumber=0, topicName=null, topicId=null, topicList=[], attachment=null, authenticateStatus=null, createdAvatar=https://wx.qlogo.cn/mmopen/jW482SpianMayicTRbRZ5RzaiabIFicf63hKvVMjL6aJlx4yX4UcXmzX9DyibCRcicq0QtCRWMaQKh8MYjE1D3EKUBopgiaGWYuqbeR/0, createdBy=0c2b1999806, createdName=三生有幸9135, createdTime=Sat Oct 21 12:50:44 CST 2017, time=2017-10-21, status=1, ipAttribution=), GetPortalCommentsPageByObjectIdResponse(id=254465, encodeId=9e00254465cb, content=谢谢分享, beContent=null, objectType=article, channel=null, level=null, likeNumber=57, replyNumber=0, topicName=null, topicId=null, topicList=[], attachment=null, authenticateStatus=null, createdAvatar=https://wx.qlogo.cn/mmopen/Pw2csslt7CukWiabqiblnQAXaDEiaxhu025c3P0XshccTrbvGWBjKvnHIxbK3vqa80P7WGIFuicCFet97TicrNKpgB3TdabxP1vMh/0, createdBy=28851960965, createdName=榄枷檬, createdTime=Fri Oct 20 07:01:49 CST 2017, time=2017-10-20, status=1, ipAttribution=), GetPortalCommentsPageByObjectIdResponse(id=254438, encodeId=c38d254438a2, content=学习了新知识.受益, beContent=null, objectType=article, channel=null, level=null, likeNumber=51, replyNumber=0, topicName=null, topicId=null, topicList=[], attachment=null, authenticateStatus=null, createdAvatar=https://cdnapi.center.medsci.cn/medsci/head/2017/08/29/bbc5cc0eed9b8d17623d2fd49dbdf19a.jpg, createdBy=79522135794, createdName=yjs木玉, createdTime=Fri Oct 20 05:46:28 CST 2017, time=2017-10-20, status=1, ipAttribution=), GetPortalCommentsPageByObjectIdResponse(id=254433, encodeId=d3b3254433d4, content=使用热熔垂直加压充填时.需要考虑到根管封闭适应性以及热应用持续时间., beContent=null, objectType=article, channel=null, level=null, likeNumber=59, replyNumber=0, topicName=null, topicId=null, topicList=[], attachment=null, authenticateStatus=null, createdAvatar=https://cdnapi.center.medsci.cn/medsci/head/2017/04/24/1c2dbd6706e64df33befd6663f1d6b37.jpg, createdBy=94f61661779, createdName=lyh994, createdTime=Fri Oct 20 02:23:38 CST 2017, time=2017-10-20, status=1, ipAttribution=), GetPortalCommentsPageByObjectIdResponse(id=254411, encodeId=e654254411b7, content=不错的视频值得推荐一下, beContent=null, objectType=article, channel=null, level=null, likeNumber=51, replyNumber=0, topicName=null, topicId=null, topicList=[], attachment=null, authenticateStatus=null, createdAvatar=, createdBy=04f22055142, createdName=131****2916, createdTime=Thu Oct 19 23:03:06 CST 2017, time=2017-10-19, status=1, ipAttribution=)]
    2017-10-20 yjs木玉

    学习了新知识.受益

    0

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    2017-10-20 lyh994

    使用热熔垂直加压充填时.需要考虑到根管封闭适应性以及热应用持续时间.

    0

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    2017-10-19 131****2916

    不错的视频值得推荐一下

    0